Investigation of Trandolapril
Martin
Vickers
9th December 2008
Experimental Data
Click image to access powder diffraction data (.spf format)
Chemical Name
(2S,3aR,7aS)-1-[(2S)-2-[[(2S)-1-ethoxy-1-oxo-4-phenylbutan-2-yl]amino]propanoyl]-2,3,3a,4,5,6,7,7a-octahydroindole-2-carboxylic
acid
Chemical Formula
C24H34N2O5 |
|
Preparation and Instrumentation Parameters
- Stoe StadiP transmission (capillary) Powder Diffractometer
- Cu Kα1 radiation
- Pre-sample germanium monochromator
- 40kV/30mA generator power
- Linear Position Sensitive Detector 6° 2θ range
- Rotating 0.6mm sample capillary
- uncrushed, unsieved sample
- NBS Silicon (111 reflection) calibration
- Data aquisition details:
- Date collected: 08/12/08
- File: ST3369.RAW
- ×2 ranges from 2 to 40° 2θ
- PSD step: 0.2°
- Count Time: 150 seconds per step
- Binning: 4 channels per point
- Data Step: 0.02°
Results
- Indexed using Lzon
- Refined lattice parameters by Lebail fit:
| Unit Cell Lengths (Å): |
|
a 15.068(1) |
b 19.764(1) |
c 7.671(1) |
| Unit Cell Angles (°): |
|
α 90 |
β 90 |
γ 90 |
| Unit Cell Volume (Ų): |
| 2284 |
- Z: 4
- System: Orthorhombic
- Possible Space Group: P212121
Reference