Experimental Data

Click image to access powder diffraction data (.spf format)

Chemical Name

S(+)-2-ethoxy-4-[N-{1-(2-piperidinophenyl)-3-methyl-1-butyl}aminocarbonylmethyl]benzoic acid

Chemical Formula

C27H36N2O4

Preparation and Instrumentation Parameters

• Stoe StadiP transmission (capillary) Powder Diffractometer
• Co Kα1 X-ray radiation
• Pre-sample germanium monochromator
• 40kV/30mA generator power
• Linear Position Sensitive Detector 6° 2θ range
• Rotating 0.5mm sample capillary
• sieved 100μm, uncrushed sample
• NBS Silicon (111 reflection) calibration
• Data aquisition details:
• Date collected: 07/12/05
• File: ST1456.RAW
• Range from 2 to 40° 2θ
• PSD step: 0.1°
• Count Time: 90 seconds per step
• Binning: 4 channels per point
• Data Step: 0.02°

• Indexed using KOHL
• Refined lattice parameters by Lebail fit:

	Unit Cell Lengths (Å):		a 25.916(1)	b 9.668(1)	c 21.640(1)
	Unit Cell Angles (°):		α 90	β 105.319(1)	γ 90
	Unit Cell Volume (Ų):		5230

• Z: 8
• System: Monoclinic
• Possible Space Group: C2

Reference

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