Experimental Data

Click image to access powder diffraction data (.spf format)

Chemical Name

(1R,2S)-2-(aminomethyl)-N,N-diethyl-1-phenylcyclopropanecarboxamide hydrochloride

Chemical Formula

C15H22N2O .HCl

Preparation and Instrumentation Parameters

• Stoe StadiP transmission (capillary) Powder Diffractometer
• Cu Kα1 radiation
• Pre-sample germanium monochromator
• 40kV/30mA generator power
• Linear Position Sensitive Detector 6° 2θ range
• Rotating 0.5mm sample capillary
• crushed, sieved 100μm sample
• NBS Silicon (111 reflection) calibration
• Data aquisition details:
• Date collected: 09/12/08
• File: ST3457.RAW
• ×2 ranges from 2 to 30° 2θ
• PSD step: 0.2°
• Count Time: 150 seconds per step
• Binning: 4 channels per point
• Data Step: 0.02°

• Indexed using ITO12
• Refined lattice parameters by Lebail fit:

	Unit Cell Lengths (Å):		a 12.350(1)	b 29.687(1)	c 9.027(1)
	Unit Cell Angles (°):		α 90	β 90	γ 90
	Unit Cell Volume (Ų):		3310

• Z: 4
• System: Orthorhombic
• Possible Space Group: PCCN

Reference