Experimental Data

Click image to access powder diffraction data (.spf format)

Chemical Name

(3S)-N-methyl-3-naphthalen-1-yloxy-3-thiophen-2-ylpropan-1-amine hydrochloride

Chemical Formula

C18H19NOS · HCl

Preparation and Instrumentation Parameters

• Stoe StadiP transmission (capillary) Powder Diffractometer
• Cu Kα1 X-ray radiation
• Pre-sample germanium monochromator
• 40kV/30mA generator power
• Linear Position Sensitive Detector 6° 2θ range
• Rotating 0.6mm sample capillary
• uncrushed, unsieved sample
• NBS Silicon (111 reflection) calibration
• Data aquisition details:
• Date collected: 04/07/2008
• File: ST2989.RAW
• ×2 ranges from 2 to 40° 2θ
• PSD step: 0.2°
• Count Time: 140 seconds per step
• Binning: 4 channels per point
• Data Step: 0.02°

• Indexed using ITO12
• Refined lattice parameters by Lebail fit:

	Unit Cell Lengths (Å):		a 13.588(1)	b 6.956(1)	c 9.816(1)
	Unit Cell Angles (°):		α 90	β 110.002(2)	γ 90
	Unit Cell Volume (Ų):		872

• Z: 2
• System: Monoclinic
• Possible Space Group: P2₁

Reference

EP1934197