Experimental Data

Click image to access powder diffraction data (.spf format)

Chemical Name

1-benzyl-4-[(5,6-dimethoxy-1-indanon)-2-yl] methylpiperidine hydrochloride

Chemical Formula

C24H29NO3 · HCl

Preparation and Instrumentation Parameters

• Stoe StadiP transmission (capillary) Powder Diffractometer
• Cu Kα1 X-ray radiation
• Pre-sample germanium monochromator
• 40kV/30mA generator power
• Linear Position Sensitive Detector 6° 2θ range
• Rotating 0.5mm sample capillary
• uncrushed, unsieved sample
• NBS Silicon (111 reflection) calibration
• Data aquisition details:
• Date collected: 17/12/04
• File: ST1219.RAW
• from 5 to 35° 2θ
• PSD step: 0.1°
• Count Time: 90 seconds per step
• Binning: 4 channels per point
• Data Step: 0.02°

• Indexed using ITO12
• Refined lattice parameters by Lebail fit:

	Unit Cell Lengths (Å):		a 14.353(1)	b 11.836(1)	c 13.555(1)
	Unit Cell Angles (°):		α 90	β 107.729(3)	γ 90
	Unit Cell Volume (Ų):		2193

• Z: 4
• System: Monoclinic
• Possible Space Group: P2₁/c

Reference

European Patent EP1211243