This page was updated 16^th December 2008 to include a fuller range data set

Experimental Data

Click image to access powder diffraction data (.spf format)

Chemical Name

7-[4-[4-(2,3-dichlorophenyl)-1- piperazinyl]butoxy]-3,4-dihydrocarbostyril

Chemical Formula

C23H27Cl2N3O2

Preparation and Instrumentation Parameters

• Stoe StadiP transmission (capillary) Powder Diffractometer
• Cu Kα1 X-ray radiation
• Pre-sample germanium monochromator
• 40kV/30mA generator power
• Linear Position Sensitive Detector 6° 2θ range
• Rotating 0.5mm sample capillary
• sieved 100μm, uncrushed sample
• NBS Silicon (111 reflection) calibration
• Data aquisition details:
• Date collected: 15/12/08
• File: ST3387.RAW. Replaces ST1432.RAW
• ×2 ranges from 2 to 45° 2θ and summed
• PSD step: 0.2°
• Count Time: 160 seconds per step
• Binning: 4 channels per point
• Data Step: 0.02°

• Indexed using TREOR90
• Refined lattice parameters by Lebail fit:

	Unit Cell Lengths (Å):		a 10.195(1)	b 12.163(1)	c 18.750(1)
	Unit Cell Angles (°):		α 82.171(2)	β 97.533(3)	γ 97.143(3)
	Unit Cell Volume (Ų):		2271

• Z: 4
• System: Triclinic
• Space Group: P1 or P-1

Reference

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